Difference between revisions of "Geochemical Analysis N Lab"

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(→‎강의 계획 Lecture schedule)
 
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{{#Customtitle:지구화학및 실험 Geochemistry & Lab}}
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{{#Customtitle:지구화학분석학 및 실험 Geochemical Analysis & Lab}}
 
<br/>
 
<br/>
  
 
== 개요 Outlines ==
 
== 개요 Outlines ==
  
−
This course is to help students understand geological processes and phenomena with the principles of chemistry.  The knowledge from this class will certainly be the basis of learning almost all fields of geology, and thus it is one of the essential courses which geology and other neighbour major students should take.
+
Will learn the basic theories of chemical analysis in a classroom and practice the actual geochemical analyses in a laboratory.
 
      
 
      
  
−
== 일반 과목 정보 Gneral course information ==
+
== 일반 과목 정보 General course information ==
  
−
* Course code: 330016
+
* Course code: 330053
−
* Credit-Lecture-Lab work: 3-2-2
+
* Credit-Lecture-Lab work: 3-2-3
 
* Grading: With Midterm Exam (30%) + Final Exam (30%) + Lab work (30%) + Attendance (10%)
 
* Grading: With Midterm Exam (30%) + Final Exam (30%) + Lab work (30%) + Attendance (10%)
 
* Type of class: Lecture + Discussion + Lab work (probably solving the problems)
 
* Type of class: Lecture + Discussion + Lab work (probably solving the problems)
−
 
  
 
== 교재 및 참고서 Text & references ==
 
== 교재 및 참고서 Text & references ==
  
−
* Text: Principles and Applications of Inorganic Chemistry (G. Faure, 1991, Macmillan)
+
* Text: None
−
* References: Any inorganic geochemistry text (eg. Principles of Geochemistry by M. Moor in 1982, John Wiley)
+
* References: Any analytical chemistry or chemical analysis book will be helpful.
  
  
 
== 수강 조건 Prerequisites ==
 
== 수강 조건 Prerequisites ==
  
−
Geology and chemistry knowledge should help
+
Background in chemical analysis is highly favorable, but not "must-have".
  
  
 
== 강의 계획 Lecture schedule ==
 
== 강의 계획 Lecture schedule ==
  
−
{| border=1 cellspacing=0 cellpadding=10 bgcolor=#E9F7FE style="border:1px #000000 solid; border-collapse:collapse"
+
{| width="850" border=1 cellspacing=0 cellpadding=10 bgcolor=#E9F7FE style="border:1px #000000 solid; border-collapse:collapse"
−
| width=30 height=40 bgcolor=#B6E0FA align=center style="border:1px #000000 solid; border-collapse:collapse"| Week #
+
| bgcolor=#B6E0FA align=center style="width: 5%; border:1px #000000 solid; border-collapse:collapse"| Week No.
−
| width=300 bgcolor=#B6E0FA align=center style="border:1px #000000 solid; border-collapse:collapse"| Lecture title  
+
| bgcolor=#B6E0FA align=center style="width: 25%; border:1px #000000 solid; border-collapse:collapse"| Lecture title  
−
| width=200 bgcolor=#B6E0FA align=center style="border:1px #000000 solid; border-collapse:collapse"| Assignments
+
| bgcolor=#B6E0FA align=center style="width: 25%; border:1px #000000 solid; border-collapse:collapse"| Assignment
−
| width=150 bgcolor=#B6E0FA align=center style="border:1px #000000 solid; border-collapse:collapse"| Lecture note
+
| bgcolor=#B6E0FA align=center style="width: 15%; border:1px #000000 solid; border-collapse:collapse"| Lecture note
−
| width=150 bgcolor=#B6E0FA align=center style="border:1px #000000 solid; border-collapse:collapse"| Reading Materials<br/>& Others
+
| bgcolor=#B6E0FA align=center style="width: 30%; border:1px #000000 solid; border-collapse:collapse"| Reading Materials<br/>& Other Supplements
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 1
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 1
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Definition of Geochemistry, Various Fields of Study in Geochemistry
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| What is Geochemical Analysis?
 +
Introduction of the course and lecture plan
 +
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Student grouping (2-3 students a group)
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_Course_information.pptx|Course Information]]
 +
* [[media:GA_introduction_kr.pptx|교과목 개요]]
 +
* [[media:GA_Ch1.pptx|Ch.1]]
 +
* [[media:GA_Ch1_kr.pptx|제 1장]]
 +
<br>
 +
* [[media:GA_EXP1.docx| Experiment 1]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| [[file:Chapter01_WM_White.pdf‎]]
+
* [[media:Lab_note_1.jpg| Lab note ex. 1]]
 +
* [[media:Lab_note_2.jpg| Lab note ex. 2]]
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 2
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 2
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Solar system and elemental distribution
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Classification of chemical analysis
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Thinking of how the elements distributes as they do now
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Preliminary survey on the sampling area
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_Ch2.pptx|Ch.2]]
 +
* [[media:GA_Ch2_kr.pptx|제 2장]]
 +
<br>
 +
* [[media:GA_EXP2.docx| Experiment 2]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 3
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 3
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Thermodynamics for geochemistry, Part 1
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Errors in a chemical analysis
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Surveying the characteristics of the Moon
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Preparation for the sampling
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_EXP3.docx| Experiment 3]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:handylab-pH-11_manual.pdf| pH meter manual]]
 +
* [[media:handylab-LF-11_manual.pdf| Conductvity meter manual]]
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 4
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 4
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Thermodynamics for geochemistry, Part 2
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Sample collection and treatments
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| What is chemical equilibrium?
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Statistical estimation of the analytical errors
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_Ch3.ppt|Ch.3]]
 +
* [[media:GA_Ch3_kr.pptx|제 3장]]
 +
<br>
 +
* [[media:GA_EXP4.docx| Experiment 4]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:water_record.hwp| Water log form]]
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 5
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 5
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Structure of atoms; how the electron configuration controls the properties of the elements
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| On-site measurements on water samples: pH, Eh, K(25), T, etc
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Calculation of the Gibbs free energy change as a function of temperature and pressure
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Sampling design (Reporting the sampling design for one's own graduation thesis area)
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_Ch4.pptx|Ch.4]]
 +
* [[media:GA_Ch4_kr.pptx|제 4장]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [http://chemwiki.ucdavis.edu/Analytical_Chemistry/Analytical_Chemistry_2.0/11_Electrochemical_Methods/11B_Potentiometric_Methods Chemwiki-Potentiometric method page]
 +
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 6
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 6
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Chemical bondings and crystal chemistry of minerals
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Analyses of water samples:  Acidity & alkalinity, IC, UV-VIS
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Calculation of ionicities of bondings in various silicates
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* Sample collection/treatment and on-site measurements
 +
* Reading the manuals of all the instruments for the measurements
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_Ch5_kr.pptx|제 5장]]
 +
<br>
 +
* [[media:GA_EXP5.docx| Experiment 5]]
 +
* [[media:GA_EXP6.docx| Experiment 6]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:alkalinity_USGS.pdf| USGS Alkalinity titration method]]
 +
* [http://www.clas.ufl.edu/users/jbmartin/Hydrologic_Processes/2nd_problem_set/Gran_titration.html gran titration]
 +
* [http://en.wikipedia.org/wiki/Gran_plot Wikipedia Gran plot page]
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 7
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 7
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  Radiogenic isotopes, Part 1; principles of radioactive decay and age dating
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  Analyse of water samples: Major and minor constituents (ICP-AES & ICP-MS)
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Caculation of Radius ratio range for a given coordination number
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Alkalinity measurement
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_Ch6-1_kr.pptx|제 6장 - 1]]
 +
* [[media:GA_Ch6-2_kr.pptx|제 6장 - 2]]
 +
* [[media:GA_Ch6-3_kr.pptx|제 6장 - 3]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:Basic_Theories_IC.pdf|IC 기본 원리]]
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 8
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 8
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Radiogenic isotopes, Part 2; utilization of radiogenic isotopes in various geologic fields
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Midterm exam
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Determination of absolute age
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Si measurements
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_EXP7.docx| Experiment 7]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [http://www.caslab.com/EPA-Methods/PDF/EPA-Method-3701.pdf EPA spectrometric Si determination]
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 9
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 9
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Stable isotopes, Part 1; isotope fractionation
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Evaluation of analysis results
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Fe(II)/Fe(III) measurements
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:GA_EXP8.docx| Experiment 8]]
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 +
* [[media:Std_Methods-3500-Fe.pdf| Phenanthroline method]]
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 10
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 10
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Stable isotopes, Part 2; Utilization of stable isotopes in various geological fields
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Analyses of rock and soil samples: Sample disintegration
−
 
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Anionic constituent measurements
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Calculation of isotope fractionation
 
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 11
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 11
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Igeneous geochemistry, Part 1: Major element distribution
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Analyses of rock and soil samples: Classical methods
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Extraction for stable isotope analysis
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Cationic constituents measurements
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 12
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 12
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Igneous geochemistry, Part 2: Minor elelment distribution
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Analyses of rock and soil samples: Nondestructive instrumental analyses
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Interpretation of stability diagrams
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Equilibrium modeling
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 13
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 13
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Low T aqueous geochemistry, Part 1; types of reactions and equilibrium
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Analyses of rock and soil samples: Destructive instrumental analyses
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Analysis of REE patterns
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Final report preparation
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 14
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 14
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Low T aqueous geochemistry, Part 2; Phase equilibria
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Other analyses: Isotopic, structural, organic, atmospheric analyses
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Calculation of solubilities
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Presentation
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
|-
 
|-
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 15
 
| align=center style="border:1px #222222 solid; border-collapse:collapse"| 15
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Low T aqueous geochemistry, Part 3; Redox reactions
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Final Exam
−
| align=left style="border:1px #000000 solid; border-collapse:collapse"| Eh-pH diagram
+
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
−
 
 
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
| align=left style="border:1px #000000 solid; border-collapse:collapse"|  
 
|}
 
|}
 +
<br />
  
 
== 유용한 링크 Helpful links ==
 
== 유용한 링크 Helpful links ==
  
−
[http://www.korearth.net/lecture/geochem/gchem_intro/contents.php KorEArtH Geochemistry Lecture]
+
[http://www.korearth.net/lecture/geochem/gchem_anal/contents.php KorEArtH Geochemical Analysis Lecture]

Latest revision as of 21:23, 2 December 2015

{{#Customtitle:지구화학분석학 및 실험 Geochemical Analysis & Lab}}

개요 Outlines

Will learn the basic theories of chemical analysis in a classroom and practice the actual geochemical analyses in a laboratory.


일반 과목 정보 General course information

  • Course code: 330053
  • Credit-Lecture-Lab work: 3-2-3
  • Grading: With Midterm Exam (30%) + Final Exam (30%) + Lab work (30%) + Attendance (10%)
  • Type of class: Lecture + Discussion + Lab work (probably solving the problems)

교재 및 참고서 Text & references

  • Text: None
  • References: Any analytical chemistry or chemical analysis book will be helpful.


수강 조건 Prerequisites

Background in chemical analysis is highly favorable, but not "must-have".


강의 계획 Lecture schedule

Week No. Lecture title Assignment Lecture note Reading Materials
& Other Supplements
1 What is Geochemical Analysis?

Introduction of the course and lecture plan

Student grouping (2-3 students a group)


2 Classification of chemical analysis Preliminary survey on the sampling area


3 Errors in a chemical analysis Preparation for the sampling
4 Sample collection and treatments Statistical estimation of the analytical errors


5 On-site measurements on water samples: pH, Eh, K(25), T, etc Sampling design (Reporting the sampling design for one's own graduation thesis area)
6 Analyses of water samples: Acidity & alkalinity, IC, UV-VIS
  • Sample collection/treatment and on-site measurements
  • Reading the manuals of all the instruments for the measurements


7 Analyse of water samples: Major and minor constituents (ICP-AES & ICP-MS) Alkalinity measurement
8 Midterm exam Si measurements
9 Evaluation of analysis results Fe(II)/Fe(III) measurements
10 Analyses of rock and soil samples: Sample disintegration Anionic constituent measurements
11 Analyses of rock and soil samples: Classical methods Cationic constituents measurements
12 Analyses of rock and soil samples: Nondestructive instrumental analyses Equilibrium modeling
13 Analyses of rock and soil samples: Destructive instrumental analyses Final report preparation
14 Other analyses: Isotopic, structural, organic, atmospheric analyses Presentation
15 Final Exam


유용한 링크 Helpful links

KorEArtH Geochemical Analysis Lecture

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